Environmental Analysis II.

Környezetvédelmi analitika II

A tantárgyleírás hatályossága

Hatályosság kezdete:

2026. March 21.

Hatályosság vége:

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Subject name (Hungarian, English)

Környezetvédelmi analitika II

Environmental Analysis II.

Subject code

BMEVESAM108

Subject type

—

Training Level

—

Course types and hours (weekly/semester)

Course type	lecture	tutorial	laboratory
hours (weekly)	2	0	1
type (linked/independent)	—	—	derived course

Assessment type

vizsga

Credits

Subject coordinator

Horváth Viola

position: egyetemi docens

contact: horvath.viola@vbk.bme.hu

Responsible department

Szervetlen és Analitikai Kémia Tanszék

Faculty

Vegyészmérnöki és Biomérnöki Kar

Subject website

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Primary curriculum type

—

Direct prerequisites – Strong prerequisite

none

Direct prerequisites – Weak prerequisite

none

Direct prerequisites – Parallel prerequisite

none

Direct prerequisites – Milestone prerequisite

none

Direct prerequisites – Exclusion

none

Objectives

Programme

6. 1. GC-MS techniques, speacial aspects on capabilities of low and high resolution mass spectrometry. Designing separations and interpretaion of GC-MS data.

- Advantages of hyphenated (multidimensional) techniques. GC-MS, GC-FTIR, GC-ICP, compared to GC-FID, GC-TID, GC-ECD, GC-FPD and GC-PID. Lecturer: Jenő Fekete

- Advantages of GCxGC compared to one dimensional GC. GCxGC-FID and GCxGC-ToF. Application of the methods to food contaminants. Data interpretation. Lecturer: Jenő Fekete

- High resolution techniques (HRGC-HRMS) and their advantages compared to low resolution GC-MS. Applications in food analysis. Lecturer: Jenő Fekete

- Ion sources: electron ionization and chemical ionization. Lecturer: Jenő Fekete

- Use of spectrum libraries. Lecturer: Jenő Fekete

- Designing gas chromatographic measurements and its relation to sample preparation in food analysis. Lecturer: Jenő Fekete

6. 2. HPLC-MS: ionization, applications, analyzers, hybrid instruments. Prerequisities of the liquid chromatographic separations. Designing separations.

- General requirements for hyphenation of liquid chromatography and mass spectrometry. Athmospheric pressure electrospray and ionspray sources. Ionizable compounds. Lecturer: Jenő Fekete

- Athmospheric pressure chemical ionization (APCI) and photoionization (APPI) and their applications in food analyis and other industries. Other ionization techniques. Lecturer: Jenő Fekete

- Rules of designing liquid chromatographic separations. Differences in buffer systems and column choice when using HPLC-MS. Lecturer: Jenő Fekete

- Requirements for advanced sample preparation methods for HPLC-MS. Lecturer: Jenő Fekete

- HPLC-MS-MS and HPLC-MSⁿ, hybrid techniques and their operation. Lecturer: Jenő Fekete

- Designing separation for HPLC-MS and HPLC-MS-MS determination of food contaminants. Lecturer: Jenő Fekete

- Fast liquid chromatography: UHPLC, HTLC, monolith columns and applications in food control. Lecturer: Jenő Fekete

6. 3. Other hyphenated techniques

- CE-MS: challenges of coupling CE to MS. Advantages and disadvantages compared to HPLC-MS. Introduction to method development. Lecturer: Sándor Tömösközi

- SFC-MS: advantages and disadvantages compared to HPLC-MS and GC-MS. Lecturer: Jenő Fekete

- HPLC-NMR: current opinion and possible future trends. Lecturer: Jenő Fekete

- Advanced separation technologies in food analysis. Affinity separation methods: capillary chromatography and affinity CE. Common electrophoretic techniques and their applications in practice. Lecturer: Sándor Tömösközi

The subject lays emphasis on the applications of modern separation methods, especially on hyphenated techniques. The use of this applications is neccesary in the field of environmental protection, pharmaceutical industry, food industry, clinical biochemistry and synthetic industry.

Learning outcomes

Ez a tantárgy a KKK rendeletben meghatározott, következő kompetenciák fejlesztését szolgálja:

Knowledge

No learning outcomes recorded.

Skills

No learning outcomes recorded.

Attitudes

No learning outcomes recorded.

Autonomy and responsibility

No learning outcomes recorded.

Oktatási módszertan

lectures and laboratory practices

Tanulástámogató anyagok

Online források

1. Fekete J.: A környezetvédelmi analitika alapjai, Jáva-98 Kft., Budapest, 2003.; 2. Fekete J.: Folyadékkromatográfia, Edisonhouse, Kft. Budapest, 2006,; 3. Fekete J.:A folyadékkromatográfia fejlsesztési irányai, Merck Kft, Budapest, 2008; 4. Kőmíves J.(szerk.): Környezeti analitika (Phare jegyzet), Műegyetemi Kiadó, Budapest, 1997.; 5. S. F. Y. Li: Capillary Electroforesis , Journal of Chromatography Library, Vol. 52, Elsevier Science Publ. B.V., Amsterdam, 1993.

Recommended preliminary knowledge for completing the subject

Knowledge type competencies

(azon előzetes ismeretek összessége, amelyek megléte nem kötelező, de a tantárgy eredményes teljesítését nagyban elősegíti)

nincs

Skill type competencies

(azon előzetes képességek és készségek összessége, amelyek megléte nem kötelező, de a tantárgy eredményes teljesítését nagyban elősegíti)

nincs

Recommended (non-compulsory) preliminary competencies

(azon ajánlott (nem kötelező) előzetesen megszerzendő kompetenciák összessége, amelyek jelentősen hozzájárulnak a tantárgy eredményes teljesítéséhez)

Basics of classical and instrumental analysis methods, general biochemical and chromatography knowledge.

General rules

Requirements: Writing a test after the lab practices and written exam. Re-takes: The test can be repeated. Consultations: By previously fixed appointment with the lecturer.

Assessment methods

In-term assessments

No detailed assessments provided.

Weight of in-term assessments

No weights provided.

Exam-period assessments

No detailed assessments provided.

Weight of exam elements

No weights provided.

Grade calculation

No grade thresholds provided.

Attendance requirements

No attendance requirements provided.

Rules for retake and resubmission

Not provided.

Short description

Not provided.

Detailed description

Name: Post: Department: Dr. Jenő Fekete professor emeritus Dept. of Inorg. and Anal. Chem.

Recommended courses

12 hours for laboratory work and 25 for preparation for the test and exam.

Workload to complete the subject

No workload breakdown provided.

Validity of subject requirements

Requirements valid from:

—

Requirements valid until:

—

Curriculum placement

Faculty	Program	Curriculum	Curriculum type	Primary
Default Faculty	környezetmérnöki	Környezetmérnöki mesterképzési szak tanterve	kötelező	nem
Default Faculty	környezetmérnöki	Környezetmérnöki mesterképzési szak tanterve	kötelező	nem
Default Faculty	Default Program	Default Curriculum	—	nem